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Beilstein J. Org. Chem. 2015, 11, 1469–1474, doi:10.3762/bjoc.11.159
Graphical Abstract
Figure 1: DCPD (1) and ruthenium benzylidene catalyst 2.
Scheme 1: ROMP of dicyclopentadiene by a ruthenium alkylidene initiator.
Figure 2: Top: DSC plot of PDCPD 24 hours after polymerization. Blue line: 1st heating–cooling cycle. Black l...
Figure 3: Change in Tg for a representative PDCPD sample as a function of time.
Figure 4: Intensity of exothermic peak as a function of rest time at room temperature for different samples.
Figure 5: Peak intensity as function of age. Samples were analyzed every two weeks. The abnormal low intensit...
Figure 6: Resting temperature effect. Blue columns: resting at room temperature. Orange columns: resting at −...
Figure 7: Top: Sample after 1 week with ethyl vinyl ether. Bottom: Sample after 1 week with diethyl ether.